Policeman (laboratory): Difference between revisions
Adding short description: "Plastic scraper" |
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{{Short description|Plastic scraper}} |
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[[Image:Rubberpoliceman.jpg|right|thumb|Rubber policemen]] |
[[Image:Rubberpoliceman.jpg|right|thumb|Rubber policemen]] |
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A '''policeman''' is a hand-held flexible natural-rubber or plastic scraper. The common type of it is attached to a glass rod and used in [[chemical]] [[laboratories]] to transfer residues of [[precipitate]] or solid on glass surfaces when performing [[gravimetric analysis]]. This equipment works well under gentle, delicate and precise requirement. A policeman also comes in various sizes, shapes, and types. Some of them come in one-piece flexible plastic version and some in stainless. The origin of the policeman and its name cannot be identified for sure but some clues led back to the 19th century from |
A '''policeman''' is a hand-held flexible natural-rubber or plastic scraper. The common type of it is attached to a glass rod and used in [[chemical]] [[laboratories]] to transfer residues of [[precipitate]] or solid on glass surfaces when performing [[gravimetric analysis]]. This equipment works well under gentle, delicate and precise requirement. A policeman also comes in various sizes, shapes, and types. Some of them come in one-piece flexible plastic version and some in stainless. The origin of the policeman and its name cannot be identified for sure but some clues led back to the 19th century from German chemist [[Carl Remigius Fresenius]]. |
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⚫ | In chemistry, [[gravimetric analysis]] is essential. After precipitating the chemical element of interest, successfully |
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⚫ | Then rubber policeman also recorded in 1910 edition of J. C. |
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* It likes police that protected the beaker from scratching. |
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⚫ | The second speculation is the most likely the one since in the 1937 edition of |
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== Structure == |
== Structure == |
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A policeman is generally a flexible natural-rubber attached to a |
A policeman is generally a flexible natural-rubber blade attached to a glass rod, which is typically 5 mm to 6 mm diameter and 150 mm long. However, it also comes in various sizes and shapes depending on its uses. The rubber material provides chemical resistance. In some designs, there is no glass rod, but instead the whole item is made of plastic or stainless steel and is shaped into a spatula or scraper shape at the end. |
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== Uses == |
== Uses == |
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A policeman can be used for cleaning the inside of glassware, or for getting the last bit of precipitate out of a vessel. Especially in chemical laboratories it often |
[[File:The use of a plastic policeman.webm|thumb|The use of a plastics policeman for raking the precipitate on the beaker wall]]A policeman can be used for cleaning the inside of glassware, or for getting the last bit of precipitate out of a vessel. Especially in chemical laboratories it is often used to transfer residues of precipitate or solid on glass surfaces when performing the gravimetric analysis. <br>It also used in biological laboratories, to transfer tissue culture cells from a plate to a suspension. It feature is to prevent the glass rod from scratching or breaking glassware. |
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It also used in biological laboratories, to transfer tissue culture cells from a plate to a suspension. Their feature is to prevent the glass rod from scratching or breaking glassware. |
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[[|thumb|The example use of plastics policeman for raking the precipitate on the beaker wall]] |
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* It is like the police in that it protects the beaker from scratching.<ref name="Jensen">{{cite journal |last1=Jensen |first1=William B |author1-link=William B. Jensen |date=2008 |title=The Origin of the Rubber Policeman |url=http://www.che.uc.edu/jensen/w.%20b.%20jensen/reprints/146.%20Rubber%20Policeman.pdf |journal=Journal of Chemical Education |volume=85 |issue=776 |page=776 |bibcode=2008JChEd..85..776J |doi=10.1021/ed085p776 |access-date=13 October 2017}}</ref> |
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⚫ | In chemistry, [[gravimetric analysis]] is essential. After precipitating the chemical element of interest, successfully transferring all of the [[precipitate]] to the [[filtration]] funnel for separation from the supernatant liquid is required. This can be done by using a stream of distilled water from a [[wash bottle]]. This is less effective because dense precipitates may become compacted at the bottom of the beaker, while light precipitates may be dispersed on the walls of the beaker. A glass rod can be used to remove the precipitate but this risks poking a hole in the bottom of the beaker or scratching the beaker wall. In the 19th century, German chemist, [[Carl Remigius Fresenius]] suggested a solution to overcome this problem using a device similar to the rubber policeman.<ref name="Jensen" /> |
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⚫ | Then rubber policeman was also recorded in 1910 edition of J. C. Olsen's textbook of quantitative analysis that states ''"''particles adhering to the glass must be removed by means of a so-called policeman, which is made by inserting the end of a rather thick large-sized glass stirring-rod into a short piece of rubber tubing. The rubber tube should be left protruding slightly beyond the end of the glass tube and sealed together with a little bicycle [i.e. rubber] cement."''<ref name="Jensen" />'' |
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== Applications == |
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These are some examples of the experiment that use the policeman. |
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=== Gravimetric Analysis of a Soluble Chloride === |
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The experiment intends to introduce the student to the technique called Gravimetric Analysis by using the Chloride as an example. This technique helps determine amount of an analyte by the measurement of mass.<ref>{{cite web|title=Gravimetric Analysis|url=http://www.wiredchemist.com/chemistry/instructional/laboratory-tutorials/gravimetric-analysis|website=WeirdChemist|accessdate=13 October 2017}}</ref>The policeman uses here to scrape down any of the precipitates that have dried on the sides of the beaker or the glass stirring rod, so that 100% of the precipitate will be used for the Gravimetric Analysis<ref>{{cite web|title=Gravimetric Analysis of a Soluble Chloride|url=http://www.chem.uky.edu/courses/che226/Labs/020-Gravim_Cl.pdf|publisher=University of Kentucky|accessdate=13 October 2017}}</ref> |
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=== Isolation of Casein from Milk === |
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The policeman can be used for stirring the mixture in the fragile containers and for draining the solid substance. As in the experiment called Isolation of Casein from milk which has the objective to isolate chemical substances found in milk. A policeman uses to stir the mixture of milk and acetic acid. Then it uses to push the casein up onto the side of the beaker so that most liquid drains from the solid.<ref>{{cite book|last1=Pavis|first1=Donald L.|last2=Lampman|first2=Gary M.|last3=Kris|first3=George S.|title=Introduction to Organic Laboratory Techniques: A Small Scale Approach|date=2005|publisher=Davis Haris|location=Belmount, CA, USA|isbn=0534408338|page=464|edition=2|accessdate=13 October 2017}}</ref> |
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⚫ | The second speculation is the most likely the one since in the 1937 edition of Hackh's Chemical Dictionary "platinum policeman," defined as "a platinum-iridium claw that fits over a glass rod and is used to hold a quantitative filter during ignition,"<ref>{{cite book |last1=Hackh |first1=Ingo Waldemar Dagobert |title=Hackh's chemical dictionary: containing the words generally used in chemistry |last2=Grant |first2=Julius |date=1937 |publisher=P. Blakiston's son & co., inc. |location=The University of California |page=564}}</ref> which the purpose of the policeman was to prevent the escape of stray filter paper from the crucible during the ignition process that causes thermal updrafts from the burner. Therefore, for policeman, it likely means to prevent the escape of stray precipitate. |
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=== Cell Lysates Preparation === |
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In the cell lysates preparation, it requires a very gentle procedure for preparing them after [[transfection]] of cells growing in well plates. The policeman which is soft and flexible uses for a scrape or detach those cells for transferring or observe. |
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<ref>{{cite book|last1=Deb|first1=Sumitra|last2=Deb|first2=Swati Palit|title=Methods in Molecular Biology|date=2003|publisher=Humana Press Inc.|location=Totowa, New Jersey|isbn=1588291065|page=98|accessdate=13 October 2017}}</ref> |
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== See also == |
== See also == |
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* [[Glass rod]] |
* [[Glass rod]] |
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* [[Spatula]] |
* [[Spatula]] |
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* [[Beaker]] |
* [[Beaker (glassware)|Beaker]] |
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=References= |
==References== |
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{{Reflist}} |
{{Reflist}} |
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{{Laboratory equipment}} |
{{Laboratory equipment}} |
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[[Category:Laboratory equipment]] |
[[Category:Laboratory equipment]] |
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[[Category:Microbiology equipment]] |
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[[Category:Chemical equipment]] |
Latest revision as of 15:52, 10 June 2024
A policeman is a hand-held flexible natural-rubber or plastic scraper. The common type of it is attached to a glass rod and used in chemical laboratories to transfer residues of precipitate or solid on glass surfaces when performing gravimetric analysis. This equipment works well under gentle, delicate and precise requirement. A policeman also comes in various sizes, shapes, and types. Some of them come in one-piece flexible plastic version and some in stainless. The origin of the policeman and its name cannot be identified for sure but some clues led back to the 19th century from German chemist Carl Remigius Fresenius.
Structure
[edit]A policeman is generally a flexible natural-rubber blade attached to a glass rod, which is typically 5 mm to 6 mm diameter and 150 mm long. However, it also comes in various sizes and shapes depending on its uses. The rubber material provides chemical resistance. In some designs, there is no glass rod, but instead the whole item is made of plastic or stainless steel and is shaped into a spatula or scraper shape at the end.
Uses
[edit]A policeman can be used for cleaning the inside of glassware, or for getting the last bit of precipitate out of a vessel. Especially in chemical laboratories it is often used to transfer residues of precipitate or solid on glass surfaces when performing the gravimetric analysis.
It also used in biological laboratories, to transfer tissue culture cells from a plate to a suspension. It feature is to prevent the glass rod from scratching or breaking glassware.
Origin
[edit]There is no answer on where the name "policeman" comes from, though it may be related to the function of the instrument.
- It is like the police in that it protects the beaker from scratching.[1]
- It is like the police in that it gathers up any stray or escaped particles of precipitate on the beaker wall.[1]
In chemistry, gravimetric analysis is essential. After precipitating the chemical element of interest, successfully transferring all of the precipitate to the filtration funnel for separation from the supernatant liquid is required. This can be done by using a stream of distilled water from a wash bottle. This is less effective because dense precipitates may become compacted at the bottom of the beaker, while light precipitates may be dispersed on the walls of the beaker. A glass rod can be used to remove the precipitate but this risks poking a hole in the bottom of the beaker or scratching the beaker wall. In the 19th century, German chemist, Carl Remigius Fresenius suggested a solution to overcome this problem using a device similar to the rubber policeman.[1]
Then rubber policeman was also recorded in 1910 edition of J. C. Olsen's textbook of quantitative analysis that states "particles adhering to the glass must be removed by means of a so-called policeman, which is made by inserting the end of a rather thick large-sized glass stirring-rod into a short piece of rubber tubing. The rubber tube should be left protruding slightly beyond the end of the glass tube and sealed together with a little bicycle [i.e. rubber] cement."[1]
However, it seems that Olsen has nothing to do with the mass production and sales of this invention. Instead, Oesper Collections catalog indicated that Henry Heil Company of St. Louis sold policemen as early as 1904.[1]
The second speculation is the most likely the one since in the 1937 edition of Hackh's Chemical Dictionary "platinum policeman," defined as "a platinum-iridium claw that fits over a glass rod and is used to hold a quantitative filter during ignition,"[2] which the purpose of the policeman was to prevent the escape of stray filter paper from the crucible during the ignition process that causes thermal updrafts from the burner. Therefore, for policeman, it likely means to prevent the escape of stray precipitate.
See also
[edit]References
[edit]- ^ a b c d e Jensen, William B (2008). "The Origin of the Rubber Policeman" (PDF). Journal of Chemical Education. 85 (776): 776. Bibcode:2008JChEd..85..776J. doi:10.1021/ed085p776. Retrieved 13 October 2017.
- ^ Hackh, Ingo Waldemar Dagobert; Grant, Julius (1937). Hackh's chemical dictionary: containing the words generally used in chemistry. The University of California: P. Blakiston's son & co., inc. p. 564.