Knoop hardness test: Difference between revisions

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Angles of a Knoop hardness test indenter

The Knoop hardness test /kəˈnuːp/ is a microhardness test – a test for mechanical hardness used particularly for very brittle materials or thin sheets, where only a small indentation may be made for testing purposes. A pyramidal diamond point is pressed into the polished surface of the test material with a known (often 100 g) load, for a specified dwell time, and the resulting indentation is measured using a microscope. The geometry of this indenter is an extended pyramid with the length to width ratio being 7:1 and respective face angles are 172 degrees for the long edge and 130 degrees for the short edge. The depth of the indentation can be approximated as 1/30 of the long dimension.^[1] The Knoop hardness HK or KHN is then given by the formula:

Sample values
Material	HK
Dentin	68
Gold foil	69
Tooth enamel	343
Quartz	820
Silicon carbide	2480
Diamond	7000

HK={{{\text{load}}(\mathrm {kgf} )} \over {{\text{impression area}}(\mathrm {mm} ^{2})}}={P \over {C_{\text{p}}L^{2}}}

where:

L is the length of indentation along its long axis

C_p is the correction factor related to the shape of the indenter, ideally 0.070279

P is the load

HK values are typically in the range from 100 to 1000, when specified in the conventional units of kg_f⋅mm⁻². The SI unit, pascal, is sometimes used instead: 1 kg_f⋅mm⁻² = 9.80665 MPa.

The test was developed by Frederick Knoop^[2] and colleagues at the National Bureau of Standards (now NIST) of the United States in 1939, and is defined by the ASTM E384 standard.

The advantages of the test are that only a very small sample of material is required, and that it is valid for a wide range of test forces. The main disadvantages are the difficulty of using a microscope to measure the indentation (with an accuracy of 0.5 micrometre), and the time needed to prepare the sample and apply the indenter.

Variables such as load, temperature, and environment, may affect this procedure, which have been examined in detail.^[3]

References

^ "Microhardness Test", Surface Engineering Forum
^ F. Knoop, C.G. Peters and W.B. Emerson (1939). "A Sensitive Pyramidal-Diamond Tool for Indentation Measurements". Journal of Research of the National Bureau of Standards. 23 (1): 39–61 (Research Paper RP1220). doi:10.6028/jres.023.022.
^ Czemuska, J. T. (1984). Proc. Br. Ceram. Soc. 34: 145–156. {{cite journal}}: Missing or empty |title= (help)

External links

[1] "Microhardness Test", Surface Engineering Forum

[2] F. Knoop, C.G. Peters and W.B. Emerson (1939). "A Sensitive Pyramidal-Diamond Tool for Indentation Measurements". Journal of Research of the National Bureau of Standards. 23 (1): 39–61 (Research Paper RP1220). doi:10.6028/jres.023.022.

[3] Czemuska, J. T. (1984). Proc. Br. Ceram. Soc. 34: 145–156. {{cite journal}}: Missing or empty |title= (help)

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[2]

[3]

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+[[File:Knoop_hardness_test_indenter.svg|thumb|300px|Angles of a Knoop hardness test indenter]]
-The '''Knoop hardness test''' is a microhardness test - a test for mechanical [[hardness]] used particularly for very brittle materials or thin sheets, where only a small indentation may be made for testing purposes. A [[pyramid]]al [[diamond]] point is pressed into the polished surface of the test material with a known force, for a specified dwell time, and the resulting indentation is measured using a [[microscope]]. The Knoop hardness ''HK'' or ''KHN'' is then given by the formula:
+The '''Knoop hardness test''' {{IPAc-en|k|ə|ˈ|n|uː|p}} is a microhardness test – a test for mechanical [[hardness]] used particularly for very brittle materials or thin sheets, where only a small indentation may be made for testing purposes. A [[pyramid]]al [[diamond]] point is pressed into the polished surface of the test material with a known (often 100&nbsp;g) load, for a specified dwell time, and the resulting indentation is measured using a [[microscope]]. The geometry of this indenter is an extended pyramid with the length to width ratio being 7:1 and respective face angles are 172 degrees for the long edge and 130  degrees for the short edge. The depth of the indentation can be approximated as 1/30 of the long dimension.<ref>[http://www.gordonengland.co.uk/hardness/microhardness.htm "Microhardness Test", Surface Engineering Forum]</ref> The Knoop hardness ''HK'' or '''''KHN''''' is then given by the formula:
+[[File:Knoop-and Mohs- scale.svg|thumb|250px|Comparison between the Mohs and the Knoop scales]]
-:<math>HK={{load(\mbox{kgf})} \over {impression\ area (\mbox{mm}^2)}}={P \over {C_pL^2}}</math>
-where:
-:''L'' = length of indentation along its long axis
-:''C''<sub>p</sub> = correction factor related to the shape of the indenter, ideally 0.070279
-:''P'' = load
-HK values are typically in the range from 100 to 1000, when specified in the conventional units of kg<sub>f</sub>·mm<sup>-2</sup>.  The SI unit, [[pascal (unit)|pascal]]s, are sometimes used instead: 1 kg<sub>f</sub>·mm<sup>-2</sup> = 9.80665 MPa.
-The test was developed by Frederick Knoop<ref>F. Knoop, C.G. Peters and W.B. Emerson, “A Sensitive Pyramidal-Diamond Tool for Indentation Measurements,” ''Journal of Research of the National Bureau of Standards'', V23 #1, July 1939, Research Paper RP1220, p 39–61.</ref> and colleagues at the National Bureau of Standards (now [[NIST]]) of the [[USA]] in 1939, and is defined by the [[ASTM]] D1474 standard.
-The advantages of the test are that only a very small sample of material is required, and that it is valid for a wide range of test forces. The main disadvantages are the difficulty of using a microscope to measure the indentation (with an accuracy of 0.5 [[micrometre]]), and the time needed to prepare the sample and apply the indenter.
 {| class="wikitable"
 |+ Sample values
 !Material !! HK
 |-
-|[[Gold]] foil||69
+|[[Dentin]] || 68
 |-
-|[[Quartz]]||820
+|[[Gold]] foil || 69
 |-
-|[[Silicon carbide]]||2480
+|[[Tooth enamel]] || 343
 |-
-|[[Diamond]]||8000
+|[[Quartz]] || 820
+|-
+|[[Silicon carbide]] || 2480
+|-
+|[[Diamond]] || 7000
 |}
+: <math>HK={{\text{load}(\mathrm{kgf})} \over {\text{impression area} (\mathrm{mm}^2)}}={P \over {C_\text{p}L^2}}</math>
+where:
+: ''L'' is the length of indentation along its long axis
+: ''C''<sub>p</sub> is the correction factor related to the shape of the indenter, ideally 0.070279
+: ''P'' is the load
+HK values are typically in the range from 100 to 1000, when specified in the conventional units of kg<sub>f</sub>⋅mm<sup>−2</sup>.  The SI unit, [[pascal (unit)|pascal]], is sometimes used instead: 1&nbsp;kg<sub>f</sub>⋅mm<sup>−2</sup> = 9.80665&nbsp;MPa.
+The test was developed by [[Frederick Knoop]]<ref>{{cite journal|author=F. Knoop, C.G. Peters and W.B. Emerson|title=A Sensitive Pyramidal-Diamond Tool for Indentation Measurements|journal=Journal of Research of the National Bureau of Standards|volume=23|issue=1|year=1939| pages=39–61 (Research Paper RP1220)|url=https://archive.org/details/jresv23n1p39|doi=10.6028/jres.023.022|doi-access=free}}</ref> and colleagues at the National Bureau of Standards (now [[NIST]]) of the United States in 1939, and is defined by the [[ASTM]] E384 standard.
+The advantages of the test are that only a very small sample of material is required, and that it is valid for a wide range of test forces. The main disadvantages are the difficulty of using a microscope to measure the indentation (with an accuracy of 0.5 [[micrometre]]), and the time needed to prepare the sample and apply the indenter.
+Variables such as load, temperature, and environment, may affect this procedure, which have been examined in detail.<ref>{{cite journal|last=Czemuska|first=J. T.|journal=Proc. Br. Ceram. Soc.|year=1984|volume=34|pages=145–156}}</ref>
 == See also ==
+{{Div col}}
 * [[Vickers hardness test]]
-* [[Ceramography#Microindention Hardness and Toughness|Knoop hardness of ceramics]]
+* [[Ceramography#Microindentation hardness and toughness|Knoop hardness of ceramics]]
+* [[Leeb Rebound Hardness Test]]
+* [[Meyer hardness test]]
+{{Div col end}}
-==References==
+== References ==
 {{reflist}}
 == External links ==
 * [http://www.efunda.com/units/hardness/convert_hardness.cfm?cat=Steel&HD=HK efunda]
+* [https://web.archive.org/web/20080113233200/http://www.lib.umich.edu/dentlib/Dental_tables/Knoophard.html Dental hardness tables]
 [[Category:Hardness tests]]
 [[de:Härte#Härteprüfung nach Knoop]]
-[[fr:Échelle de Knoop]]
-[[ja:ヌープ硬度]]
-[[it:Scala di Knoop]]
-[[pt:Dureza Knoop]]
-[[sv:Knoop-provning]]